I always hit issues

I had everything rusting for about 6 hours. Then let it go 4 more.
I ran out of distilled water so I asked my wife to pick up some. The only stuff she could find was the Wegmans branded distilled water.
It came out of boiling still very much red. It also didn't card off well. It took a lot of manual rubbing.
I wonder if this is bad distilled water.
The picture of the frame is before boiling.
The picture of the hammer is after boiling.
The pics of everything is after carding.





